Coordination Compounds of Yttrium(III) with Urea and Dimethylacetamide: Composition, Structure, Thermal Behavior

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Coordination compounds of yttrium(III) nitrate with urea (Ur) and N,N-dimethylacetamide, [Y(H2O)(Ur)2(NO3)3] (I), [Y(Ur)3(NO3)3] (II) and [Y(DMAA)3(NO3)3] (III), were synthesized; their compositions, structural features and thermolysis were studied with the use of elemental analysis, IR spectroscopy, X-ray powder and single-crystal diffraction, thermal gravimetric analysis, differential scanning calorimetry. The coordination compounds can be used for the synthesis of nano-scale yttrium(III) oxide.

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Sobre autores

E. Bettels

MIREA — Russian Technological University

Email: savinkina@mirea.ru
Rússia, Moscow, 119571

M. Polukhin

MIREA — Russian Technological University

Email: savinkina@mirea.ru
Rússia, Moscow, 119571

I. Karavaev

MIREA — Russian Technological University

Email: savinkina@mirea.ru
Rússia, Moscow, 119571

E. Savinkina

MIREA — Russian Technological University

Autor responsável pela correspondência
Email: savinkina@mirea.ru
Rússia, Moscow, 119571

G. Buzanov

Kurnakov Institute of General and Inorganic Chemistry

Email: savinkina@mirea.ru
Rússia, Moscow, 119991

A. Kubasov

Kurnakov Institute of General and Inorganic Chemistry

Email: savinkina@mirea.ru
Rússia, Moscow, 119991

V. Retivov

Kurchatov Institute National Research Center

Email: savinkina@mirea.ru
Rússia, Moscow, 123182

Bibliografia

  1. Hao S.J., Wang C., Liu Т. L. et al. // Int. J. Hydrogen. Energy. 2017. V. 42. P. 29949. https://doi.org/10.1016/j.ijhydene.2017.08.143
  2. Cho G.Y., Yu W., Lee Y.H. et al. // Int. J. Precis. Eng. Manuf.-Green Technol. 2020. V. 7. P. 423. https://doi.org/10.1007/s40684-019-00082-9
  3. Сарин В.А., Буш А.А. // Тонкие химические технологии. 2021. Т. 16. № 2. С. 55.
  4. Pan C., Huang B.H., Fan C. et al. // Rare Metals. 2020. V. 40. P. 1785. https://doi.org/10.1007/s12598-020-01475-5
  5. Gao W., Wen D., Ho I.C., Qu Y. // Mater. Today Chem. 2019. V. 12. P. 266. https://doi.org/10.1016/j.mtchem.2019.02.002
  6. Zhang R., Tu Z.A., Meng S. et al. // Rare Metals. 2023. V. 42. P. 176. https://doi.org/10.1007/s12598-022-02136-5
  7. Shimoda N., Kimura Y., Kobayashi Y. et al. // Int. J. Hydrogen. Energy. 2017. V. 42. P. 29745. https://doi.org/10.1016/j.ijhydene.2017.10.108
  8. Hao J., Studenikin S.A., Cocivera M. // J. Lumin. 2001. V. 93. P. 313. https://doi.org/10.1016/S0022-2313(01)00207-1
  9. Diego-Rucabado A., Segura A., Aguado F. et al. // J. Lumin. 2022. V. 252. P. 119378. https://doi.org/10.1016/j.jlumin.2022.119378
  10. Hasabeldaim E., Swart H.C., Kroon R.E. // Phys. B: Condens. Matter. 2023. V. 671. P. 415417. https://doi.org/10.1016/j.physb.2023.415417
  11. Bernard-Granger G., Guizard C., San-Miguel L. // J.Am. Ceram. Soc. 2007. V. 90. № 9. P. 2698. https://doi.org/10.1111/j.1551-2916.2007.01759.x
  12. Saratale R.G., Karuppusamy I., Saratale G.D. et al. // Colloids Surf., B. 2018. V. 180. P. 20. https://doi.org/10.1016/j.colsurfb.2018.05.045
  13. Rajakumar G., Mao L., Bao T. et al. // Appl. Sci. 2021. V. 11. № 5. P. 2172. https://doi.org/10.3390/app11052172
  14. Kannan S.K., Sundrarajan M. // Bull. Mater. Sci. 2015. V. 38. P. 945. https://doi.org/10.1007/s12034-015-0927-7
  15. Nagajyothi P.C., Pandurangan M., Veerappan M. et al. // Mater. Lett. 2018. V. 216. P. 58. https://doi.org/10.1016/j.matlet.2017.12.081
  16. Mariano-Torres J.A., Lopez-Marure A., Garcia-Hernandez M. et al. // Mater. Trans. 2018. V. 59. № 12. P. 1915. https://doi.org/10.2320/matertrans.M2018248
  17. Gaponov A.V. // Phys. B: Condens. Matter. 2022. V. 639. P. 414010. https://doi.org/10.1016/j.physb.2022.414010
  18. Li N., Yanagisawa K. // J. Solid State Chem. 2008. V. 181. № 8. P. 1738. https://doi.org/10.1016/j.jssc.2008.03.031
  19. Abdulghani A.J., Al-Ogedy W.M. // Iraqi J. Sci. 2015. V. 56. № 2. P. 1572.
  20. Levashov E.A., Mukasyan A.S., Rogachev A.S., Shtansky D.V. // Int. Mater. Rev. 2017. V. 62. № 4. P. 203. https://doi.org/10.1080/09506608.2016.1243291
  21. Gizowska M., Piatek M., Perkowski K. et al. // Nanomater. 2020. V. 10. № 5. P. 831. https://doi.org/10.3390/nano10050831
  22. Chen K., Peng J., Srinivasakannan C. et al. // J. Alloys Compd. 2018. V. 742. P. 13. https://doi.org/10.1016/j.jallcom.2018.01.258
  23. Savinkina E.V., Karavaev I.A., Grigoriev M.S. et al. // Inorg. Chim. Acta. 2022. V. 532. P. 120759. https://doi.org/10.1016/j.ica.2021.120759
  24. Savinkina E.V., Karavaev I.A., Grigoriev M.S. // Polyhedron. 2020. V. 192. P. 114875. https://doi.org/10.1016/j.poly.2020.114875
  25. Караваев И.А., Савинкина Е.В., Григорьев М.С. и др. // Журн. неорган. химии. 2020. Т. 67. № 8. С. 1080.
  26. Петричко М.И., Караваев И.А., Савинкина Е.В. и др. // Журн. неорган. химии. 2023. Т. 68. № 4. С. 482.
  27. Mangalaja R.V., Mouzon J., Hedstrom P. et al. // Powder Technol. 2009. V. 191. № 3. P. 309. https://doi.org/10.1016/j.powtec.2008.10.019
  28. Ryskaliyeva A.K., Baltbayev M.E., Zhubatova A.M. // Acta. Chim. Slov. 2018. V. 65. P. 127. https://doi.org/10.17344/acsi.2017.3683
  29. Koslowski N., Hoffmann R.C., Trouillet V. et al. // RSC Adv. 2019. V. 9. P. 31386. https://doi.org/10.1039/C9RA05348D
  30. Худайбергенова Н., Сулайманкулов К. // Журн. неорган. химии. 1981. Т. 26. С. 1156.
  31. Bruker, SAINT, Bruker AXS Inc., Madison, WI, 2018.
  32. Krause L., Herbst-Irmer R., Sheldrick G.M., Stalke D. // J. Appl. Crystallogr. 2015. V. 48. № 1. P. 3. https://doi.org/10.1107/S1600576714022985
  33. Sheldrick G.M. // Acta Crystallogr., Sect. C: Struct. Chem. 2015. V. 71. P. 3. https://doi.org/10.1107/S2053229614024218
  34. Dolomanov O.V., Bourhis L.J., Gildea R.J. et al. // J. Appl. Crystallogr. 2009. V. 42. P. 339 https://doi.org/10.1107/S0021889808042726
  35. Накамото К. // ИК-спектры и спектры КР неорганических и координационных соединений. М.: Мир, 1991.
  36. Hay B.P., Hancock R.D. // Coord. Chem. Rev. 2001. V. 21. № 1. P. 61. https://doi.org/10.1016/S0010-8545(00)00366-0
  37. Hay B.P., Clement O., Sandrone G., Dixon D.A. // Inorg. Chem. 1998. V. 37. № 22. P. 5887. https://doi.org/10.1021/ic980641j
  38. Schaber P.M., Colson J., Higgins S. et al. // Thermochim. Acta. 2004. V. 424. P. 131. https://doi.org/10.1016/j.tca.2004.05.018

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2. Appendix
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3. Scheme 1. Scheme for the synthesis of complex compounds I, II and III.

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4. Fig. 1. Diffractograms of precursors and isolated complexes: 1 - Ur, 2 - Y(NO3)3 - 6H2O, 3 - III (exp.), 4 - III (theor.), 5 - I (exp.), 6 - I (theor.), 7 - II (exp.), 8 - II (theor.).

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5. Fig. 2. Molecular structures of complexes I (a), II (b), III (c).

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6. Fig. 3. Thermograms of complexes I (a) and III (b) in air; 1 - mass loss curve, 2 - differential curve.

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7. Fig. 4. Diffraction patterns of Y2O3 preparations obtained by annealing complexes III (1), I (2), II (3) in air.

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